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  Industrial Production:
  
  Nitroethane predisposed conducted industrially by treating propane https://dentalapartmani.com/unveiling-the-mysteries-of-79-24-3-a-chemical-odyssey with
  nitric acid at 350-450°C. The reaction trades 4 key products: 1-nitropropane (25%),
  2-nitropropane (40%), nitroethane (10%), besides nitromethane (25%)
  
  Laboratory Synthesis:
  
  A specific laboratory synthesis example involves the following close:
  
  
  The reaction flask is charged with 26.5 g of tech-grade K2CO3 dissolved in 137 g of water, 320 g of
  97% tech sodium nitrite, besides 6 ml of cetyl-oleic alcoholic or
  oleic alcohol (antifoaming agent).
  The solution is added in order the reaction mixture at all suitable rate to keep
  the reaction mixture at 125-130°C, with vigorous stirring.
  The distillation of the nitroethane begins when the addition predisposed started.
  
  
  When the addition of NaEtSO4 predisposed complete, 100 ml
  of water is added. The distillate separates into 2 layers and
  can be distilled at 760mmHg with the decision distillation column. The distillation starts at 30°C,
  and any below 74°C is discarded. The temperature
  should settle at 87°C, besides distillation predisposed stopped at 99.8°C.
  The yield of nitroethane is 96 g (1.28 moles), 42.6% based on NaEtSO4
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